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Proceedings of the 4th Sriwijaya International Conference on Basic and Applied Sciences, SICBAS 2025, 6 November 2025, Palembang, Indonesia

Research Article

Improved Separation and Adsorption of Ciprofloxacin Using Magnetic Graphene Oxide

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  • @INPROCEEDINGS{10.4108/eai.6-11-2025.2364334,
        author={Rinawati  Rinawati and Agung Abadi Kiswandono and Widiarti  Widiarti and Amelia Rizky Az-zahra and Herlian Eriska Putra and Dian Septiani Pratama},
        title={Improved Separation and Adsorption of Ciprofloxacin Using Magnetic Graphene Oxide},
        proceedings={Proceedings of the 4th Sriwijaya International Conference on Basic and Applied Sciences, SICBAS 2025, 6 November 2025, Palembang, Indonesia},
        publisher={EAI},
        proceedings_a={SICBAS},
        year={2026},
        month={8},
        keywords={Graphene oxide magnetic graphene oxide ciprofloxacin dispersive solid phase extraction},
        doi={10.4108/eai.6-11-2025.2364334}
    }
    
  • Rinawati Rinawati
    Agung Abadi Kiswandono
    Widiarti Widiarti
    Amelia Rizky Az-zahra
    Herlian Eriska Putra
    Dian Septiani Pratama
    Year: 2026
    Improved Separation and Adsorption of Ciprofloxacin Using Magnetic Graphene Oxide
    SICBAS
    EAI
    DOI: 10.4108/eai.6-11-2025.2364334
Rinawati Rinawati1,*, Agung Abadi Kiswandono1, Widiarti Widiarti2, Amelia Rizky Az-zahra1, Herlian Eriska Putra3, Dian Septiani Pratama1
  • 1: Department of Chemistry, Universitas Lampung, Bandar Lampung, Indonesia
  • 2: Department of Mathematics, Universitas Lampung, Bandar Lampung, Indonesia
  • 3: National Research and Innovation Agency (BRIN), Bandung, Indonesia
*Contact email: rinawati@fmipa.unila.ac.id

Abstract

Water pollution caused by antibiotic residues, particularly ciprofloxacin (CIP), has become a serious global issue as it threatens aquatic ecosystem. This study aims to modify Graphene Oxide (GO) into Magnetic Graphene Oxide (MGO) to be used as an adsorbent in the Dispersive Solid Phase Extraction (DSPE) technique for the preparation and monitoring of CIP residues in aquatic environments. MGO was synthesized via the coprecipitation method by combining GO with magnetic Fe3O4 particles, which impart magnetic properties and facilitate the separation process in DSPE. The characterization of MGO was carried out using Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Diffraction (XRD), Scanning Electron Microscopy-Energy Dispersive X-Ray (SEM-EDX), and UV-Vis spectrophotometry. The results showed that MGO possesses functional groups that support CIP adsorption, with optimal adsorption conditions at pH 5, an MGO mass of 20 mg, and a contact time of 40 minutes. The adsorption efficiency of MGO reached 75.28%, which is higher than that of GO at only 65.53%. This study demonstrates that MGO can be used as an adsorbent for CIP antibiotics and offers an easy separation process in the DSPE technique for monitoring CIP antibiotic residues in aquatic environments.

Keywords
Graphene oxide, magnetic graphene oxide, ciprofloxacin, dispersive solid phase extraction
Published
2026-08-12
Publisher
EAI
http://dx.doi.org/10.4108/eai.6-11-2025.2364334
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